文献类型：期刊文献

中文题名：三元乙丙橡胶的^(13)C-NMR定量分析

英文题名：Quantitative Analysis of Ethylene-Propylene-Diene Rubberby ^(13)C-NMR Spectrometry

作者：史新梅[1];潘铁英[1];王复[1];罗会俊[1];贺彩霞[1];董师孟[2];虞宇力[2]

机构：[1]华东理工大学分析测试中心,上海200237;[2]上海申雅密封件有限公司,上海200237

年份：2002

卷号：21

期号：2

起止页码：51

中文期刊名：分析测试学报

外文期刊名：Journal of Instrumental Analysis

收录：CSTPCD;;北大核心:【北大核心2000】；CSCD:【CSCD2011_2012】；

语种：中文

中文关键词：三元乙丙橡胶;乙叉降冰片烯;乙烯;核磁共振谱法;定量分析;碳13;含量测定

外文关键词：Ethylene-propylene-diene rubbers; 5 _ Ethylidene _ 2 _ norbornene; Ethylene; 13C _ NMR

摘要：用 13C核磁共振波谱法对三元乙丙橡胶进行了研究 ,通过图谱中各个峰的积分值 ,并用特定的计算公式测定了三元乙丙橡胶中乙烯及第三单体乙叉降冰片烯的含量 ,为红外光谱批量的定量分析建立了基准化的标定。
Components of ethylene-propylene-diene rubber(EPDR) were quantitatively analyzed by 13C nuclear magnetic resonance spectrometry. The contents of ethylene and 5 _ ethylidene _ 2 _ norbornene in three samples of EPDR were determined using a calculation method through the integral areas of peaks. The results of this work could be used for calibration of quantitative analysis in a large scale by infrared spectrometry.