文献类型：期刊文献

英文题名：Study on the synthesis of β-FeOOH by the microemulsion method

作者：Liang Xiaojuan[1];Yang Yuxiang[2,4];Liu Xiangnong[3];Zhu Hui[2];Ying Haiping[2];Zhou Zheyu[2];Chen Yaru[2]

机构：[1]Dalian Maritime Univ, Dalian 116021, Peoples R China;[2]E China Univ Sci & Technol, Dept Chem, Shanghai 200237, Peoples R China;[3]Yangzhou Univ, Anal Test Ctr, Yangzhou 225002, Peoples R China;[4]Nanjing Univ, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China

年份：2008

卷号：53

期号：3

起止页码：367

外文期刊名：RUSSIAN JOURNAL OF INORGANIC CHEMISTRY

收录：;EI(收录号：20081711215157);WOS:【SCI-EXPANDED(收录号:WOS:000254881700005)】；

语种：英文

外文关键词：Hydrolysis - Microemulsions - Nanoparticles - Reaction kinetics - Synthesis (chemical) - Water

摘要：Monoclinic-FeOOH with: a = 0.9981 nm, b = 0.2948 nm, n = 1.0485 nm, beta = 92.26 degrees was synthesized by the hydrolysis of FeCl3 center dot 6H(2)O in micro emulsion including NP-4, octane, water. In this paper, the various morphology and size of the nano particles under different conditions are discussed, and it is found that the optimum conditions for synthesizing acicular beta-FeOOH is that R = 6.0, [Fe3+] = 0.02 mol/L within the pH range 1.6-2.0.