文献类型：期刊文献

英文题名：A study on the synthesis of water-soluble Sb2S3

作者：Xiang, Wei-Dong[1]; Ji, Guo-Yuan[1]; Jing, Wei[2]; Yang, Yu-Xiang[2]; Liu, Xiang-Nong[3]

机构：[1] College of Chemistry and Materials Engineering, Wenzhou University, Wenzhou, Zhejiang, 325035, China; [2] Department of Chemistry, East China University of Science and Technology, 200237, China; [3] Analysis Test Center, Yangzhou University, Yangzhou, 225009, China

年份：2012

卷号：38

期号：2

起止页码：245

外文期刊名：Glass Physics and Chemistry

收录：EI(收录号：20122115051937)

语种：英文

外文关键词：Sulfur - Optical properties

摘要：Water-soluble Sb2S3 sub-microspheres were synthesized by aqueous-phase arrested precipitation using mercaptoacetic acid as capping agent and thioacetamide (TAA) as sulfur source. The effects of the experimental conditions, such as temperature, sulfur source, reactants concentration and reaction time, on the shapes, structures and properties of the products were studied. FESEM, TEM showed the products have uniform size distribution. In addition, ultraviolet-visible spectrophotometry (UV-vis) and photoluminescence (PL) showed the resulting products have excellent optical properties. ? 2012. Pleiades Publishing, Ltd.