文献类型：期刊文献

中文题名：五氯吡啶的合成工艺优化

英文题名：Optimization of synthetic technology condition for pentachloropyridine

作者：许柳松[1];曾作祥[1];薛为岚[1];吴超[1]

机构：[1]华东理工大学化工学院,上海200237

年份：2005

卷号：34

期号：1

起止页码：43

中文期刊名：应用化工

外文期刊名：Applied Chemical Industry

收录：CSTPCD;;CSCD:【CSCD_E2011_2012】；

语种：中文

中文关键词：五氯吡啶;吡啶;氯化;正交设计

外文关键词：pentachloropyridine; pyridine; chlorination; orthogonal design

摘要：对五氯吡啶的合成工艺条件采用正交设计法进行了研究。优化的条件为:气空速500h-1,液空速0.070h-1,温度610K,时间24h。五氯吡啶的收率达到96.90%。
The reaction condition for synthesizing pentachloropyridine were optimized with orthogonal design. The optimal technology condition are also determined.The result shows that the yield of pentachloropyridine is 96.90%, when gaseous phase space velocity is 500 h^(-1), liquid-phase space velocity is 0.070h^(-1), temperature is 610K,and time is 24 h.