详细信息

A sol-gel method to synthesize indium tin oxide nanoparticles    

文献类型:期刊文献

中文题名:A sol-gel method to synthesize indium tin oxide nanoparticles

英文题名:A sol-gel method to synthesize indium tin oxide nanoparticles

作者:Xiuhua Li[1];Xiujuan Xu[1];Xin Yin[1];Chunzhong Li[2];Jianrong Zhang[1]

机构:[1]Department of Chemistry, Key LaboratoryforAdvanced Materials of Ministry of Education, East China University of Science and Technology, Shanghai 200237, China;[2]Key Laboratory for Ultrafine Materials of Ministry of Education, East China University of Science and Technology, Shanghai 200237, China

年份:2011

卷号:9

期号:5

起止页码:471

中文期刊名:Particuology

外文期刊名:颗粒学报(英文版)

收录:CSTPCD;;Scopus;CSCD:【CSCD2011_2012】;

基金:supported by grants from Ph.D. Programs Foundation of Ministry of Education of China (200802511022);National Natural Science Foundation of China (50902049)

语种:英文

中文关键词:Oxide materials Ceramics Sintering Indium tin oxide

外文关键词:Oxide materials Ceramics Sintering Indium tin oxide

摘要:Transparent conductive indium tin oxide (ITO) nanoparticles were synthesized by a novel sol-gel method. Granulated indium and tin were dissolved in HNO3 and partially complexed with citric acid. A sol-gel process was induced when tertiary butyl alcohol was added dropwise to the above solution. ITO nanopartides with an average crystallite size of 18.5 nm and surface area of 32.6 m^2 ]g were obtained after the gel was heat-treated at 700 ℃, The ITO nanoparticles showed good sinterability, the starting sintering temperature decreased sharply to 900 ℃, and the 1400 ℃ sintered pellet had a density of 98.1% of theoretical density (TD).
Transparent conductive indium tin oxide (ITO) nanoparticles were synthesized by a novel sol-gel method. Granulated indium and tin were dissolved in HNO3 and partially complexed with citric acid. A sol-gel process was induced when tertiary butyl alcohol was added dropwise to the above solution. ITO nanopartides with an average crystallite size of 18.5 nm and surface area of 32.6 m^2 ]g were obtained after the gel was heat-treated at 700 ℃, The ITO nanoparticles showed good sinterability, the starting sintering temperature decreased sharply to 900 ℃, and the 1400 ℃ sintered pellet had a density of 98.1% of theoretical density (TD).

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