详细信息
A sol-gel method to synthesize indium tin oxide nanoparticles
文献类型:期刊文献
中文题名:A sol-gel method to synthesize indium tin oxide nanoparticles
英文题名:A sol-gel method to synthesize indium tin oxide nanoparticles
作者:Xiuhua Li[1];Xiujuan Xu[1];Xin Yin[1];Chunzhong Li[2];Jianrong Zhang[1]
机构:[1]Department of Chemistry, Key LaboratoryforAdvanced Materials of Ministry of Education, East China University of Science and Technology, Shanghai 200237, China;[2]Key Laboratory for Ultrafine Materials of Ministry of Education, East China University of Science and Technology, Shanghai 200237, China
年份:2011
卷号:9
期号:5
起止页码:471
中文期刊名:Particuology
外文期刊名:颗粒学报(英文版)
收录:CSTPCD;;Scopus;CSCD:【CSCD2011_2012】;
基金:supported by grants from Ph.D. Programs Foundation of Ministry of Education of China (200802511022);National Natural Science Foundation of China (50902049)
语种:英文
中文关键词:Oxide materials Ceramics Sintering Indium tin oxide
外文关键词:Oxide materials Ceramics Sintering Indium tin oxide
摘要:Transparent conductive indium tin oxide (ITO) nanoparticles were synthesized by a novel sol-gel method. Granulated indium and tin were dissolved in HNO3 and partially complexed with citric acid. A sol-gel process was induced when tertiary butyl alcohol was added dropwise to the above solution. ITO nanopartides with an average crystallite size of 18.5 nm and surface area of 32.6 m^2 ]g were obtained after the gel was heat-treated at 700 ℃, The ITO nanoparticles showed good sinterability, the starting sintering temperature decreased sharply to 900 ℃, and the 1400 ℃ sintered pellet had a density of 98.1% of theoretical density (TD).
Transparent conductive indium tin oxide (ITO) nanoparticles were synthesized by a novel sol-gel method. Granulated indium and tin were dissolved in HNO3 and partially complexed with citric acid. A sol-gel process was induced when tertiary butyl alcohol was added dropwise to the above solution. ITO nanopartides with an average crystallite size of 18.5 nm and surface area of 32.6 m^2 ]g were obtained after the gel was heat-treated at 700 ℃, The ITO nanoparticles showed good sinterability, the starting sintering temperature decreased sharply to 900 ℃, and the 1400 ℃ sintered pellet had a density of 98.1% of theoretical density (TD).
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