文献类型：期刊文献

中文题名：碳酸二甲酯羰基化合成3-氨基噁唑烷酮-2

英文题名：Synthesis of 3-Amino-2-Oxazolidone from Dimethyl Carbonate by Carbonylation Reaction

作者：朱云峰[1];田恒水[1]

机构：[1]华东理工大学化工学院,上海200237

年份：2004

卷号：24

期号：4

起止页码：23

中文期刊名：精细化工中间体

外文期刊名：Fine Chemical Intermediates

收录：CSTPCD

语种：中文

中文关键词：碳酸二甲酯;羰基化;3-氨基噁唑烷酮-2;清洁工艺

外文关键词：dimethyl carbonate;carbonylation reaction;3-amino-2-oxazolidone;clean process

摘要：开发出了3 氨基口恶唑烷酮 2的碳酸二甲酸羰基化合成清洁工艺,并考察了催化剂、原料配比、反应时间以及反应精馏等多种因素对过程的影响,从而确立了较佳的工艺条件。
A clean synthetic technology of 3-amino-2-oxazolidone was developed by carbonylation reaction between dimethyl carbonate and 2-hydroxy-ethylhydrazine.In addition, many effect factors such as catalyst, reaction ratio,reaction time and reactive distillation etc on the process were also investigated. Based in these researches, the optimal process condition was determined.