文献类型：期刊文献

中文题名：液相法三相甲醇合成催化剂研制

英文题名：Study on Preparation of Catalyst for Three phase Methanol Synthesis

作者：薛从军[1];潘天舒[1];姚佩芳[1];房鼎业[1];朱炳辰[1]

机构：[1]华东理工大学化学工程系

年份：1997

卷号：23

期号：3

起止页码：259

中文期刊名：华东理工大学学报（自然科学版）

外文期刊名：Journal of East China University of Science and Technology

收录：CSTPCD;;EI(收录号：1997123980602);Scopus;北大核心:【北大核心1996】；CSCD:【CSCD2011_2012】；

基金：国家科委"八五"科技攻关课题

语种：中文

中文关键词：液相法;甲醇;合成;催化剂;三相床

外文关键词：liquid phase; methanol; synthesis; catalyst; three phase reactor

摘要：简述了三相床甲醇合成技术及其对催化剂的要求；考察了三相床甲醇合成催化剂的制备条件（一定的活性组分和助催化剂，沉淀温度为５０°Ｃ，干燥温度为１７０°Ｃ，焙烧温度为３５０°Ｃ，沉淀终点ｐＨ值在８．０，催化剂成型二次压片），得到活性较高、耐磨性能较好的ＴＰＭ－１型催化剂，并给出了该催化剂的孔分布数据。
The technology of three phase methanol synthesis is discussed in brief and the requirement of a catalyst is presented. A brief review of the progress of the study of catalyst preparation for three phase methanol synthesis is given. The preparation conditions of the catalyst is investigated. The conditions: determined are suitable composition of copper, zinc and promoter, coprecipitation temperature 50°C ,dry temperature 170°C, calcination temperature 350°C, and the pH value at the end of coprecipitation 8.0. A higher active and higher attrition resistant catalyst named TPM 1 is obtained. The data of pore distribution is also given.