文献类型：专利

英文题名：Method for preparing 9-(diethoxy phosphoryl methoxy ethyl)-adenine

作者：SEHN Y;WANG C;REN X;YE C;YE B

机构：[1]UNIV EAST CHINA SCI & TECHNOLOGY

申请号：CN1850831-A

申请日：2006-05-26

公开日：2006-10-25

语种：英文

收录：DERWENT

摘要：NOVELTY - This invention relates to 9-(biethoxy phosphoryl methoxyl ethyl)-adenine gland piaolin preparation method. ADVANTAGE - Comparing to existing technique, this invention simplifies preparation methods, and reduces operation cost. Furthermore, it is friendly to environment. DETAILED DESCRIPTION - (1) Materials are paraformaldehyde, 2-chlorohydrin, diethyl phosphate and dry chlorine hydride gas, they are reacted for 6-8 hours at 90-125 degree centigrade under condition of anhydrous aluminium chloride existing, and then biethoxy phosphoryl methoxyl ethyl is got after decompressionand distillation. (2) The biethoxy phosphoryl methoxyl ethyl made in (1) is condensed reacted with gland piaolin to get the object.