文献类型：专利

英文题名：Polybrominated diphenyl ethers detecting method, involves obtaining temperature of sample, filtering organic film to obtain to-be-analyzed sample, and performing mass spectrometric detection operation to obtain negative chemical ion source

作者：CHEN L;DENG J;GUO J;HUANG K;LI J;LIN K;LIU Y;XU F;ZHANG R;ZHOU P;ZHANG W;ZHOU X;FU X;LIU K;CHEN X;LIU G;LI H;LIANG J;LIANG S;LIU R;PENG H;WANG J;ZHANG G;ZHANG L;ZHANG Y;ZHANG Z;ZHAO L;ZHOU D;SIMA J;WEN D;WANG Y;XU K;YAO Z

机构：[1]UNIV EAST CHINA SCI & TECHNOLOGY

申请号：CN103235062-A

申请日：2013-04-19

公开日：2013-08-07

语种：英文

收录：DERWENT

摘要：NOVELTY - The method involves obtaining a sample with certain temperature. The sample is extracted by organic solvent. A sulfuric acid layer is removed. The sample is concentrated and dissolved to obtain chromatography liquid. The solvent is added into the chromatography liquid. An organic film is filtered to obtain a to-be-analyzed sample. Mass spectrometric detection operation is performed to obtain a negative chemical ion source. Temperature of the chemical ion source is maintained for about 150-200 degrees centigrade. Cutting time and filament ignition time of the ion source are about 3-6 minutes. USE - Polybrominated diphenyl ethers detecting method. ADVANTAGE - The method enables improving detection sensitivity and stability and ensuring qualitative and quantitative diphenyl ether residue food safety monitoring performance in a reliable manner. DESCRIPTION OF DRAWING(S) - The drawing shows a graph illustrating relationship between polybrominated diphenyl ethers detecting characteristics. '(Drawing includes non-English language text)'