文献类型：期刊文献

英文题名：Mechanochemical organic synthesis in a rotary evaporator beyond conventional application: Proof-of-concept reactions

作者：Wang, Weifeng[1];Peng, Yanqing[1]

机构：[1]East China Univ Sci & Technol, Sch Pharm, Shanghai Key Lab Chem Biol, Shanghai 200237, Peoples R China

年份：2023

卷号：53

期号：9

起止页码：625

外文期刊名：SYNTHETIC COMMUNICATIONS

收录：;EI(收录号：20242616345193);WOS:【SCI-EXPANDED(收录号:WOS:000948785400001)】；

基金：This work was financially supported by the National Key Research and Development Plan (Grant No. 2017YFD0200504).

语种：英文

外文关键词：Ball milling; mechanochemistry; rotary evaporator; solvent-free; synthesis

摘要：A novel and economical process for mechanochemical organic synthesis by ball milling performed in rotary evaporator is described. The process parameters, such as molar ratio and feeding amount of reactant, rotation frequency, as well as the number, diameter and material of the milling balls, were investigated in a model reaction. Other four test reactions were then performed using this process. The results indicated that the ball milling in rotary evaporator is practical.