成果/Result
- Effective Phosphorylation of 2,2′-Methylene-bis(4,6-di-tert-butyl) Phenol in Continuous Flow Reactors被引量：12收藏
- 作者：Yao, Hanlin Li Wan Zhao, Xiaoyu Guo, Yahui Zhou, Jian Bo, Xiaofan Mao, Yuxin Xin, Zhong
- 机构：East China Univ Sci & Technol;East China Univ Sci & Technol
- 来源：ORGANIC PROCESS RESEARCH & DEVELOPMENT 2021
- 关键词：phosphorylation reaction continuous flow synthesis precipitation clogging process optimization reactor analysis
- Thermal and Kinetic Research on a Highly Exothermic Condensation Reaction by Powerful Calorimeters被引量：9收藏
- 作者：Yao, Hanlin Wan, Li Guo, Yahui Mao, Yuxin Xin, Zhong
- 机构：East China Univ Sci & Technol;East China Univ Sci & Technol
- 来源：ORGANIC PROCESS RESEARCH & DEVELOPMENT 2022
- 关键词：2,2'-methylene-bis(4 6-di-tert-butylphenol) phosphate chloride condensation reaction calorimetry strong heat release kinetics thermal risk assessment
- Curing Kinetics of Main-Chain Benzoxazine Polymers Synthesized in Continuous Flow被引量：7收藏
- 作者：Zhou, Zhou Si, Qian Wan, Li Kuo, Shiao-Wei Zhou, Changlu Xin, Zhong
- 机构：East China Univ Sci & Technol;Natl Sun Yat Sen Univ;East China Univ Sci & Technol
- 来源：INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH 2022
- 关键词：Activation energy - Differential scanning calorimetry - Curing - Size exclusion chromatography - Kinetics - Molecular weight - Ring opening polymerization - Reaction kinetics - Nuclear magnetic resonance spectroscopy
- Zinc-Catalyzed Alkylation of Aromatic Amines in Continuous Flow被引量：5收藏
- 作者：Zhang, Le Bo, Xiaofan Yao, Hanlin Mao, Mengmei Wan, Li Xin, Zhong
- 机构：East China Univ Sci & Technol
- 来源：ORGANIC PROCESS RESEARCH & DEVELOPMENT 2020
- 关键词：4,4 '-dicumyldiphenylamine alkylation styrene continuous flow
- Development and Scale-up of the Rapid Synthesis of Triphenyl Phosphites in Continuous Flow被引量：4收藏
- 作者：Mao, Mengmei Zhang, Le Yao, Hanlin Wan, Li Xin, Zhong
- 机构：East China Univ Sci & Technol;East China Univ Sci & Technol
- 来源：ACS OMEGA 2020
- Efficient Reduction of Oxazolyl-bearing Secondary Anilides to Amines by Nickel-catalyzed Hydrosilylation被引量：2收藏
- 作者：Zhou, Jian Bo, Xiaofan Wan, Li Xin, Zhong
- 机构：East China Univ Sci & Technol;East China Univ Sci & Technol
- 来源：ASIAN JOURNAL OF ORGANIC CHEMISTRY 2020
- 关键词：nickel hydrosilylation amides oxazoline reduction
- 抗氧剂168的连续流高效制备被引量：0收藏
- 作者：茅梦梅 万力 辛忠
- 机构：华东理工大学上海市多相结构材料化学工程重点实验室;华东理工大学化工学院化学工程联合国家重点实验室
- 来源：《精细化工》 2019
- 关键词：抗氧剂168 2,4-二叔丁基苯酚 三氯化磷 连续流动 精细化工中间体
- 摘要：以2,4-二叔丁基苯酚和三氯化磷为原料,通过酯化反应连续流合成抗氧剂168,考察了反应溶剂、缚酸剂种类及用量、反应温度、反应停留时间对抗氧剂168收率的影响,并通过熔点、GC、1HNMR、13CNMR和HRMS对合成产物...
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- 溶胶-凝胶法制介孔Pd/m-TiO_(2)催化连续流Suzuki偶联反应被引量：0收藏
- 作者：薄晓帆 万力 辛忠
- 机构：华东理工大学上海市多相结构材料化学工程重点实验室;华东理工大学化工学院化学工程联合国家重点实验室
- 来源：《精细化工》 2021
- 关键词：连续流 Suzuki偶联反应 溶胶-凝胶法 介孔材料 Pd催化剂
- 摘要：以PdCl_(2)和钛酸正丁酯为原料、聚乙烯吡咯烷酮为金属保护剂、三嵌段共聚物EO_(96)PO_(70)EO_(96)为模板剂,采用溶胶-凝胶法制备了一系列不同Pd负载量(质量分数0.1%~1.0%)的非均相Pd/m-...
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